Solid-State and Super Solidus Liquid Phase Sintering of 4340 Steel SLM Powders Shaped by Fused Filament Fabrication

4340 steel powders were processed with an additive manufacturing process using the FFF (Fused Filament Fabrication) technique. A composite filament was developed to print samples and study the effect of the bed and nozzle temperatures on its physical and microstructural properties. The printed sampl...

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Main Authors: Gil-Plazas, Andres-Fernando, Rubiano-Buitrago, Julián-David, Boyacá-Mendivelso, Luis-Alejandro, Herrera-Quintero, Liz-Karen
Format: Online
Language:eng
Published: Universidad Pedagógica y Tecnológica de Colombia 2022
Subjects:
Online Access:https://revistas.uptc.edu.co/index.php/ingenieria/article/view/13913
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author Gil-Plazas, Andres-Fernando
Rubiano-Buitrago, Julián-David
Boyacá-Mendivelso, Luis-Alejandro
Herrera-Quintero, Liz-Karen
author_facet Gil-Plazas, Andres-Fernando
Rubiano-Buitrago, Julián-David
Boyacá-Mendivelso, Luis-Alejandro
Herrera-Quintero, Liz-Karen
author_sort Gil-Plazas, Andres-Fernando
collection OJS
description 4340 steel powders were processed with an additive manufacturing process using the FFF (Fused Filament Fabrication) technique. A composite filament was developed to print samples and study the effect of the bed and nozzle temperatures on its physical and microstructural properties. The printed samples were debinded and sintered by: Solid State (SS) at 1300 °C or SLPS (Supersolidus Liquid Phase Sintering) at 1420 °C. Metallography and scanning electron microscopy (SEM) identified the microstructure and phases. The hardness of the sintered samples was measured with the Vickers method. The SLPS process contributes to better densification and volume contraction; however, it promotes geometrical distortion of the samples compared to the SS samples. The microstructure of the sintered samples consists of ferrite situated in the original austenite grain and bainite. The sintering mechanism significantly influenced the hardness of the samples. Finally, a part was designed, printed, debinded, and sintered with the aim of studying the maximum inclination angle, the minimum vertical and horizontal holes, and the minimum vertical layer thickness, which can be obtained through the whole process.
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spelling oai:oai.revistas.uptc.edu.co:article-139132022-11-18T19:23:49Z Solid-State and Super Solidus Liquid Phase Sintering of 4340 Steel SLM Powders Shaped by Fused Filament Fabrication Sinterización en fase líquida super solidus y de estado sólido de polvos SLM de acero 4340 formados por fabricación de filamentos fundidos Gil-Plazas, Andres-Fernando Rubiano-Buitrago, Julián-David Boyacá-Mendivelso, Luis-Alejandro Herrera-Quintero, Liz-Karen Additive manufacturing 4340 steel debinding sintering characterization fused filament fabrication acero 4340 caracterización despolimerizado fabricación de filamentos fundidos manufactura aditiva sinterización 4340 steel powders were processed with an additive manufacturing process using the FFF (Fused Filament Fabrication) technique. A composite filament was developed to print samples and study the effect of the bed and nozzle temperatures on its physical and microstructural properties. The printed samples were debinded and sintered by: Solid State (SS) at 1300 °C or SLPS (Supersolidus Liquid Phase Sintering) at 1420 °C. Metallography and scanning electron microscopy (SEM) identified the microstructure and phases. The hardness of the sintered samples was measured with the Vickers method. The SLPS process contributes to better densification and volume contraction; however, it promotes geometrical distortion of the samples compared to the SS samples. The microstructure of the sintered samples consists of ferrite situated in the original austenite grain and bainite. The sintering mechanism significantly influenced the hardness of the samples. Finally, a part was designed, printed, debinded, and sintered with the aim of studying the maximum inclination angle, the minimum vertical and horizontal holes, and the minimum vertical layer thickness, which can be obtained through the whole process. Polvo de acero 4340 fue procesado mediante manufactura aditiva utilizando la técnica FFF (Fused Filament Fabrication). Se desarrolló un filamento compuesto para imprimir muestras y estudiar el efecto de la temperatura de la cama y de la boquilla de impresión en sus propiedades físicas y microestructurales. Las muestras impresas fueron despolimerizadas y sinterizadas en estado sólido (Solid State - SS) a 1300 °C y sinterización en fase líquida super solidus (Supersolidus Liquid Phase Sintering -SLPS) a 1420 °C. Por metalografía y microscopía electrónica de barrido (SEM) se identificó la microestructura y las fases presentes. La dureza de las muestras sinterizadas se midió con el método Vickers. El proceso SLPS contribuye a una mejor densificación y contracción volumétrica; sin embargo, promueve distorsión geométrica de las muestras en comparación con las muestras SS. La microestructura de las muestras sinterizadas consiste en ferrita situada en el límite de grano austenítico original y bainita. El mecanismo de sinterización influyó significativamente en la dureza de las muestras. Finalmente, se diseñó, imprimió, despolimerizó y sinterizó una pieza con el objetivo de estudiar el ángulo máximo de inclinación, los mínimos agujeros verticales y horizontales, y el mínimo espesor de capa vertical, que se pueden obtener a lo largo de todo el proceso. Universidad Pedagógica y Tecnológica de Colombia 2022-05-21 info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion application/pdf https://revistas.uptc.edu.co/index.php/ingenieria/article/view/13913 10.19053/01211129.v31.n60.2022.13913 Revista Facultad de Ingeniería; Vol. 31 No. 60 (2022): April-June 2022 (Continuous Publication); e13913 Revista Facultad de Ingeniería; Vol. 31 Núm. 60 (2022): Abril-Junio 2022 (Publicación Continua); e13913 2357-5328 0121-1129 eng https://revistas.uptc.edu.co/index.php/ingenieria/article/view/13913/11715 Copyright (c) 2022 Andres-Fernando Gil-Plazas, Julián-David Rubiano-Buitrago, Luis-Alejandro Boyacá-Mendivelso, Liz-Karen Herrera-Quintero http://creativecommons.org/licenses/by/4.0
spellingShingle Additive manufacturing
4340 steel
debinding
sintering
characterization
fused filament fabrication
acero 4340
caracterización
despolimerizado
fabricación de filamentos fundidos
manufactura aditiva
sinterización
Gil-Plazas, Andres-Fernando
Rubiano-Buitrago, Julián-David
Boyacá-Mendivelso, Luis-Alejandro
Herrera-Quintero, Liz-Karen
Solid-State and Super Solidus Liquid Phase Sintering of 4340 Steel SLM Powders Shaped by Fused Filament Fabrication
title Solid-State and Super Solidus Liquid Phase Sintering of 4340 Steel SLM Powders Shaped by Fused Filament Fabrication
title_alt Sinterización en fase líquida super solidus y de estado sólido de polvos SLM de acero 4340 formados por fabricación de filamentos fundidos
title_full Solid-State and Super Solidus Liquid Phase Sintering of 4340 Steel SLM Powders Shaped by Fused Filament Fabrication
title_fullStr Solid-State and Super Solidus Liquid Phase Sintering of 4340 Steel SLM Powders Shaped by Fused Filament Fabrication
title_full_unstemmed Solid-State and Super Solidus Liquid Phase Sintering of 4340 Steel SLM Powders Shaped by Fused Filament Fabrication
title_short Solid-State and Super Solidus Liquid Phase Sintering of 4340 Steel SLM Powders Shaped by Fused Filament Fabrication
title_sort solid state and super solidus liquid phase sintering of 4340 steel slm powders shaped by fused filament fabrication
topic Additive manufacturing
4340 steel
debinding
sintering
characterization
fused filament fabrication
acero 4340
caracterización
despolimerizado
fabricación de filamentos fundidos
manufactura aditiva
sinterización
topic_facet Additive manufacturing
4340 steel
debinding
sintering
characterization
fused filament fabrication
acero 4340
caracterización
despolimerizado
fabricación de filamentos fundidos
manufactura aditiva
sinterización
url https://revistas.uptc.edu.co/index.php/ingenieria/article/view/13913
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