Synthesis and characterization of Pr2S3 binary compound
In the current work it is shown that the synthesis method that consists in direct reaction of praseodymium and sulfur in its elemental form, using heat as a treatment, with relatively low temperatures and reaction time of one week, allows the preparation of Pr2S3 compound, with a purity of about 92%...
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| Format: | Online |
| Language: | spa |
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Universidad Pedagógica y Tecnológica de Colombia
2018
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| Online Access: | https://revistas.uptc.edu.co/index.php/ciencia_en_desarrollo/article/view/5974 |
| _version_ | 1801706338801156096 |
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| author | Ramírez Sanabria, Alfonso Enrique Quijano Ortega, Natalia Gaona Jurado, Sonia |
| author_facet | Ramírez Sanabria, Alfonso Enrique Quijano Ortega, Natalia Gaona Jurado, Sonia |
| author_sort | Ramírez Sanabria, Alfonso Enrique |
| collection | OJS |
| description | In the current work it is shown that the synthesis method that consists in direct reaction of praseodymium and sulfur in its elemental form, using heat as a treatment, with relatively low temperatures and reaction time of one week, allows the preparation of Pr2S3 compound, with a purity of about 92%. The respective characterization of resultant materials was carried out using powder XRD, where by it was determined that the thermal treatment used, effectively leads to the binary sulfide of interest, a compound known to be semiconductor. |
| format | Online |
| id | oai:oai.revistas.uptc.edu.co:article-5974 |
| institution | Revista Ciencia en Desarrollo |
| language | spa |
| publishDate | 2018 |
| publisher | Universidad Pedagógica y Tecnológica de Colombia |
| record_format | ojs |
| spelling | oai:oai.revistas.uptc.edu.co:article-59742022-06-15T17:03:25Z Synthesis and characterization of Pr2S3 binary compound Síntesis y caracterización del compuesto binario Pr2S3 Ramírez Sanabria, Alfonso Enrique Quijano Ortega, Natalia Gaona Jurado, Sonia tratamiento con praseodimio, tratamiento térmico, semiconductor. praseodymium sulfide, thermal treatment, semiconductor. In the current work it is shown that the synthesis method that consists in direct reaction of praseodymium and sulfur in its elemental form, using heat as a treatment, with relatively low temperatures and reaction time of one week, allows the preparation of Pr2S3 compound, with a purity of about 92%. The respective characterization of resultant materials was carried out using powder XRD, where by it was determined that the thermal treatment used, effectively leads to the binary sulfide of interest, a compound known to be semiconductor. En el trabajo actual se muestra que el método de síntesis que consiste en la reacción directa de praseodimio y azufre en su forma elemental, utiliza calor como tratamiento, con temperaturas relativamente bajas y tiempo de reacción de una semana, permite la preparación del compuesto Pr2S3, con una pureza de alrededor del 92%. La caracterización respectiva de los materiales resultantes se llevó a cabo utilizando polvo XRD, donde se determinó que el tratamiento térmico utilizado conduce de manera efectiva a la fuente binaria de interés, un compuesto conocido por ser semiconductor. Universidad Pedagógica y Tecnológica de Colombia 2018-07-04 info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion application/pdf https://revistas.uptc.edu.co/index.php/ciencia_en_desarrollo/article/view/5974 10.19053/01217488.v9.n2.2018.5974 Ciencia En Desarrollo; Vol. 9 No. 2 (2018): Vol 9, Núm. 2 (2018): Vol 9, Núm 2(2018): Julio- Diciembre; 95-98 Ciencia en Desarrollo; Vol. 9 Núm. 2 (2018): Vol 9, Núm. 2 (2018): Vol 9, Núm 2(2018): Julio- Diciembre; 95-98 2462-7658 0121-7488 spa https://revistas.uptc.edu.co/index.php/ciencia_en_desarrollo/article/view/5974/7262 Derechos de autor 2018 CIENCIA EN DESARROLLO |
| spellingShingle | tratamiento con praseodimio, tratamiento térmico, semiconductor. praseodymium sulfide, thermal treatment, semiconductor. Ramírez Sanabria, Alfonso Enrique Quijano Ortega, Natalia Gaona Jurado, Sonia Synthesis and characterization of Pr2S3 binary compound |
| title | Synthesis and characterization of Pr2S3 binary compound |
| title_alt | Síntesis y caracterización del compuesto binario Pr2S3 |
| title_full | Synthesis and characterization of Pr2S3 binary compound |
| title_fullStr | Synthesis and characterization of Pr2S3 binary compound |
| title_full_unstemmed | Synthesis and characterization of Pr2S3 binary compound |
| title_short | Synthesis and characterization of Pr2S3 binary compound |
| title_sort | synthesis and characterization of pr2s3 binary compound |
| topic | tratamiento con praseodimio, tratamiento térmico, semiconductor. praseodymium sulfide, thermal treatment, semiconductor. |
| topic_facet | tratamiento con praseodimio, tratamiento térmico, semiconductor. praseodymium sulfide, thermal treatment, semiconductor. |
| url | https://revistas.uptc.edu.co/index.php/ciencia_en_desarrollo/article/view/5974 |
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